2026-04-17T03:00:52Zhttps://riubu.ubu.es/oai/request

oai:riubu.ubu.es:10259/108702025-09-16T00:05:36Zcom_10259_9397com_10259_5087com_10259_2728col_10259_9398

Díez Carretero, Paula 2025-09-15T08:08:28Z 2025-09-15T08:08:28Z https://hdl.handle.net/10259/10870 Wheat bran and onion skin waste are agri-food by-products generated in large quantities annually. Their valorization represents an important opportunity, linked to sustainability, for obtaining bioactive compounds with beneficial properties. These by-products are notable for their high content of bioactive compounds, specifically phenolic compounds, among which quercetin and ferulic acid stand out for their antioxidant activity. The main aim of this work has been to study the technical feasibility of a combined ultrasound-assisted extraction (UAE) / nanofiltration (NF) process for the recovery of phenolic compounds present in wheat bran and onion skin wastes generated as by-products in local food companies. UAE was firstly performed for the extraction of polyphenols from wheat bran (WB) and onion skin waste (OSW) using an acetate buffer at pH 5 and an aqueous ethanol solution (70 vol. %) as solvents, respectively, under the optimum operating conditions. A final WB extract was obtained with a total polyphenol content (TPC) of 3.56 ± 0.18 mg GAE/g WB and an antioxidant activity (AA) of 7.75 ± 1.20 µmol Fe2+/g WB. An OSW extract was also obtained, with a TPC of 44.47 ± 0.83 mg GAE/g OSW, a total flavonoid concentration (TFC) of 19.22 ± 0.35 mg QE/g OSW, and an AA of 28.38 ± 2.70 mg Trolox/g OSW. Ferulic acid is the main component of wheat bran extract, while quercetin and its glycosylated derivatives are the main components of onion skin extract. Both extracts were then concentrated by nanofiltration (NF) in a high pressure stirred cell, using a NF270 flat polyamide membrane (270 Da cut-off), under optimal operating conditions reaching a volume concentration ratio (VCR) of 5 after 7,5 and 1,8 h for WB and OSW extracts, respectively, with minimal loss of polyphenols in the permeates and recoveries of AA, TPC, and TFC in the concentrates higher than 99% in all cases. The results obtained in this study could contribute to the valorization of agri-food waste using environmentally friendly techniques, demonstrating the potential o spa http://creativecommons.org/licenses/by-nc-nd/4.0/ info:eu-repo/semantics/openAccess Attribution-NonCommercial-NoDerivatives 4.0 Internacional Wheat bran Onion skin waste Polyohenols Ultrasound-assisted extraction Nanofiltration Antioxidant activity Flavonoids Ferulic acid Quercetin Recuperación de polifenoles presentes en salvado de trigo y piel de cebolla mediante un proceso combinado de extracción asistida por ultrasonidos y nanofiltración info:eu-repo/semantics/bachelorThesis