2026-04-22T15:07:37Zhttps://riubu.ubu.es/oai/requestoai:riubu.ubu.es:10259/53712022-12-20T10:33:39Zcom_10259_3924com_10259_5086com_10259_2604col_10259_3925
Arnáiz, Esther
e39de78e-c8bf-465d-b2b1-ab54e3628386
500
Moreno Mediavilla, Daniel
376
600
Quesada Pato, Roberto
458
500
0000-0003-2764-7157
2020-07-10T11:23:39Z
2020-07-10T11:23:39Z
2014-03
0003-2719
http://hdl.handle.net/10259/5371
10.1080/00032719.2013.853182
1532-236X
The extraction and determination of volatile compounds in mice urine were performed using headspace solid-phase microextraction and gas chromatography-mass spectrometry. In order to optimize the extraction conditions, experimental design was applied. A sample volume of 108 µl, a temperature of 148.6°C, and a time of 94 minutes were found to be the optimal conditions. Samples of male and female mouse urine were analyzed to determine volatile compound profiles. A total of 36 organic compounds including ketones, aldehydes, and terpenes were detected. The results revealed that compounds such as 2-isopropyl-4,5-dihydrothiazole, which is considered a male sexual pheromone, were only detected in male urine samples, whereas others like benzaldehyde were especially abundant in female mouse urine. A comparison of female samples corresponding to different stages of the estrous cycle was also performed.
European Commission ([SME-2011-1] Research for SMEs, PiedPiper project, Grant agreement: 286852)
application/pdf
spa
Taylor & Francis Group
Analytical Letters. 2014, V. 47, n. 5, p. 721-729
https://doi.org/10.1080/00032719.2013.853182
Experimental design
Gas chromatography-mass spectrometry (GC-MS)
Headspace-solid-phase micro-extraction (HS-SPME)
Mouse urine
Volatile organic compounds
Química orgánica
Chemistry, Organic
Determination of Volatiles in Mouse Urine by Headspace Solid Phase Microextraction and Gas Chromatography-Mass Spectrometry
info:eu-repo/semantics/article
info:eu-repo/semantics/acceptedVersion
info:eu-repo/semantics/openAccess
Analytical Letters
47
5
721
729
TEXT
Arnaiz-al_2014.pdf.txt
Arnaiz-al_2014.pdf.txt
Extracted text
text/plain
24084
https://riubu.ubu.es/bitstream/10259/5371/4/Arnaiz-al_2014.pdf.txt
78847bd3510ce080834c74f498f419ea
MD5
4
THUMBNAIL
Arnaiz-al_2014.pdf.jpg
Arnaiz-al_2014.pdf.jpg
IM Thumbnail
image/jpeg
2806
https://riubu.ubu.es/bitstream/10259/5371/3/Arnaiz-al_2014.pdf.jpg
63da98cc4fe396abd9cc7a6456662739
MD5
3
LICENSE
license.txt
license.txt
text/plain; charset=utf-8
999
https://riubu.ubu.es/bitstream/10259/5371/2/license.txt
b295bcbce42e2caabeb0c623d3860c06
MD5
2
ORIGINAL
Arnaiz-al_2014.pdf
Arnaiz-al_2014.pdf
application/pdf
1489431
https://riubu.ubu.es/bitstream/10259/5371/1/Arnaiz-al_2014.pdf
45cf72ea6ab7514658d9bbe669950493
MD5
1
10259/5371
oai:riubu.ubu.es:10259/5371
2022-12-20 11:33:39.428
Repositorio Institucional de la Universidad de Burgos
bubrep@ubu.es
RWwgYXV0b3IgY29tbyDDum5pY28gdGl0dWxhciBkZSBsb3MgZGVyZWNob3MgZGUgcHJvcGllZGFkIGludGVsZWN0dWFsIGRlIGxhIG9icmEsIG8gZGlzcG9uaWVuZG8gZGUgbG9zIGRlYmlkb3MgcGVybWlzb3MgZGUgbG9zIG90cm9zIHRpdHVsYXJlcywgc2kgbG9zIGh1YmllcmEsIHkgZW4gdmlydHVkIGRlIGxvcyBkZXJlY2hvcyBxdWUgbGUgY29uZmllcmUgbGEgbGVnaXNsYWNpw7NuIHZpZ2VudGUgc29icmUgcHJvcGllZGFkIGludGVsZWN0dWFsIHkgZGVyZWNob3MgZGUgYXV0b3IsIA0KQVVUT1JJWkEgYSBsYSBVbml2ZXJzaWRhZCBkZSBCdXJnb3MgYSBkaWZ1bmRpciwgZGUgbWFuZXJhIGdyYXR1aXRhLCBlbCBjb250ZW5pZG8gZGUgbG9zIGFyY2hpdm9zIGRpZ2l0YWxlcyBxdWUgY29ycmVzcG9uZGVuIGFsIGRvY3VtZW50byBkZXNjcml0byBhbnRlcmlvcm1lbnRlLCBjb24gY2Fyw6FjdGVyIG5vIGV4Y2x1c2l2byB5IGRlIG1hbmVyYSBww7pibGljYSBlbiBhY2Nlc28gYWJpZXJ0byBhIHRyYXbDqXMgZGUgSW50ZXJuZXQsIHBhcmEgbG8gcXVlIGxhIEJpYmxpb3RlY2EgcHJvY2VkZXLDoSBhIGFyY2hpdmFybG9zIGVuIGVsIFJlcG9zaXRvcmlvIEluc3RpdHVjaW9uYWwuIEFzaW1pc21vIGF1dG9yaXphIGEgbGEgVW5pdmVyc2lkYWQgZGUgQnVyZ29zIGEgcmVhbGl6YXIgbGFzIHRyYW5zZm9ybWFjaW9uZXMgbmVjZXNhcmlhcyBkZSBmb3JtYXRvLCBubyBkZSBjb250ZW5pZG8sIHBhcmEgZ2FyYW50aXphciBsYSBwcmVzZXJ2YWNpw7NuIHkgZWwgYWNjZXNvIGVuIGVsIGZ1dHVyby4NCg0KRWwgYXV0b3IgZGlzcG9uZSwgZW4gdG9kbyBjYXNvLCBkZWwgZGVyZWNobyBhIHJldm9jYXIgZXN0YSBhdXRvcml6YWNpw7NuLg0KDQpMYSBjZXNpw7NuIGRlIGRlcmVjaG9zIGRlIGVzdGEgb2JyYSBzZSBlbmN1ZW50cmEgc3VqZXRhIGEgbGEgbGVnaXNsYWNpw7NuIHZpZ2VudGUgc29icmUgcHJvcGllZGFkIGludGVsZWN0dWFsIHkgZGVyZWNob3MgZGUgYXV0b3Iu