2026-09-21T09:34:20Zhttps://riubu.ubu.es/oai/request

oai:riubu.ubu.es:10259/48582024-05-09T12:36:58Zcom_10259_4249com_10259_5086com_10259_2604col_10259_4250

Custodio Mendoza, J.A. . Carro, A.M. . Lage Yusty, M.A. . Herrero Gutiérrez, Ana Valente, Inês Maria Rodrigues, J.A. . Lorenzo, R.A. . 2018-07-20T11:12:05Z 2019-01 2020-01 0308-8146 http://hdl.handle.net/10259/4858 10.1016/j.foodchem.2018.07.100 During the industrial refining process of edible oils and the manufacture of oil-based foodstuff, contaminants such as 3-monochloropropanediol (3-MCPD) fatty acid diesters can be produced. One hundred samples of different edible oils and related fatty food purchased from local Spanish markets were analyzed to evaluate the occurrence of these contaminants. Data of seven 3-MCPD diesters together with corresponding total 3-MCPD equivalents are presented. The procedure is based on a modified QuEChERS protocol followed by LC-MS/MS analysis. Extra virgin olive oil (EVOO) and unrefined oils did not contain detectable levels of the target analytes. The highest levels of 3-MCPD diesters were found in palm oils, for 1,2-Dilinoleoyl-3-chloropropanediol (LILI) and 1–2-Bispalmitoyl-3-chloropropanediol (PAPA) with concentrations close to 10 mg kg−1 and in the lipid fraction of margarines (8.09, 3.77 and 3.72 mg kg−1 for LILI, PAPA and 1-Oleoyl-2-linoleoyl-3-chloropropanediol (OLLI), respectively). Spanish Ministry of Science and Innovation (Project AGL-2014-53647-R) and FEDER funds application/pdf eng Elsevier Food Chemistry. 2019, V. 270, p. 214-222 https://doi.org/10.1016/j.foodchem.2018.07.100 info:eu-repo/grantAgreement/MICINN/AGL-2014-53647-R Attribution-NonCommercial-NoDerivatives 4.0 International http://creativecommons.org/licenses/by-nc-nd/4.0/ info:eu-repo/semantics/openAccess 3-MCPD fatty acid diesters Edible oils Foodstuff LC-MS/MS Processing contaminants Química analítica Chemistry, Analytic Occurrence and exposure of 3-monochloropropanediol diesters in edible oils and oil-based foodstuffs from the Spanish market info:eu-repo/semantics/article info:eu-repo/semantics/acceptedVersion