<?xml version="1.0" encoding="UTF-8"?><?xml-stylesheet type="text/xsl" href="static/style.xsl"?><OAI-PMH xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/ http://www.openarchives.org/OAI/2.0/OAI-PMH.xsd"><responseDate>2026-07-30T19:48:01Z</responseDate><request verb="GetRecord" identifier="oai:riubu.ubu.es:10259/5672" metadataPrefix="mets">https://riubu.ubu.es/oai/request</request><GetRecord><record><header><identifier>oai:riubu.ubu.es:10259/5672</identifier><datestamp>2022-11-22T01:05:23Z</datestamp><setSpec>com_10259_4244</setSpec><setSpec>com_10259_5086</setSpec><setSpec>com_10259_2604</setSpec><setSpec>col_10259_4245</setSpec></header><metadata><mets xmlns="http://www.loc.gov/METS/" xmlns:doc="http://www.lyncode.com/xoai" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns:xlink="http://www.w3.org/1999/xlink" xsi:schemaLocation="http://www.loc.gov/METS/ http://www.loc.gov/standards/mets/mets.xsd" PROFILE="DSpace METS SIP Profile 1.0" TYPE="DSpace ITEM" ID="&#xa;&#x9;&#x9;&#x9;&#x9;DSpace_ITEM_10259-5672" OBJID="&#xa;&#x9;&#x9;&#x9;&#x9;hdl:10259/5672">
<metsHdr CREATEDATE="2026-07-30T21:48:01Z">
<agent TYPE="ORGANIZATION" ROLE="CUSTODIAN">
<name>Repositorio Institucional de la Universidad de Burgos</name>
</agent>
</metsHdr>
<dmdSec ID="DMD_10259_5672">
<mdWrap MDTYPE="MODS">
<xmlData xmlns:mods="http://www.loc.gov/mods/v3" xsi:schemaLocation="http://www.loc.gov/mods/v3 http://www.loc.gov/standards/mods/v3/mods-3-1.xsd">
<mods:mods xsi:schemaLocation="http://www.loc.gov/mods/v3 http://www.loc.gov/standards/mods/v3/mods-3-1.xsd">
<mods:name>
<mods:role>
<mods:roleTerm type="text">author</mods:roleTerm>
</mods:role>
<mods:namePart>Alonso Riaño, Patricia</mods:namePart>
</mods:name>
<mods:name>
<mods:role>
<mods:roleTerm type="text">author</mods:roleTerm>
</mods:role>
<mods:namePart>Sanz Díez, Mª Teresa</mods:namePart>
</mods:name>
<mods:name>
<mods:role>
<mods:roleTerm type="text">author</mods:roleTerm>
</mods:role>
<mods:namePart>Benito Román, Oscar</mods:namePart>
</mods:name>
<mods:name>
<mods:role>
<mods:roleTerm type="text">author</mods:roleTerm>
</mods:role>
<mods:namePart>Beltrán Calvo, Sagrario</mods:namePart>
</mods:name>
<mods:name>
<mods:role>
<mods:roleTerm type="text">author</mods:roleTerm>
</mods:role>
<mods:namePart>Trigueros Andrés, Ester</mods:namePart>
</mods:name>
<mods:extension>
<mods:dateAccessioned encoding="iso8601">2021-03-25T12:20:02Z</mods:dateAccessioned>
</mods:extension>
<mods:extension>
<mods:dateAvailable encoding="iso8601">2021-03-25T12:20:02Z</mods:dateAvailable>
</mods:extension>
<mods:originInfo>
<mods:dateIssued encoding="iso8601">2021-07</mods:dateIssued>
</mods:originInfo>
<mods:identifier type="issn">0308-8146</mods:identifier>
<mods:identifier type="uri">http://hdl.handle.net/10259/5672</mods:identifier>
<mods:identifier type="doi">10.1016/j.foodchem.2021.129264</mods:identifier>
<mods:abstract>The valorization of the brewer’s spent grain (BSG) generated in a craft beer industry was studied by subcritical water hydrolysis in a semi-continuous fixed-bed reactor. Temperature was varied from 125 to 185 °C at a constant flow rate of 4 mL/min. Biomass hydrolysis yielded a maximum of 78% of solubilized protein at 185 °C. Free amino acids presented a maximum level at 160 °C with a value of 55 mg free amino acids/gprotein-BSG. Polar amino acid presented a maximum at lower temperatures than non-polar amino acids. The maximum in total phenolic compounds was reached at 185 °C. This maximum is the same for aldehyde phenolic compounds such as vanillin, syringic and protocatechuic aldehyde; however, for hydroxycinnamic acids, such as ferulic acid and p-coumaric, the maximum was obtained at 160 °C. This allows a fractionation of the bioactive compounds. Subcritical water addresses opportunities for small breweries to be incorporated within the biorefinery concept.</mods:abstract>
<mods:language>
<mods:languageTerm authority="rfc3066">eng</mods:languageTerm>
</mods:language>
<mods:accessCondition type="useAndReproduction">Attribution-NonCommercial-NoDerivatives 4.0 Internacional</mods:accessCondition>
<mods:subject>
<mods:topic>Subcritical water extraction</mods:topic>
</mods:subject>
<mods:subject>
<mods:topic>Biorefinery</mods:topic>
</mods:subject>
<mods:subject>
<mods:topic>Breweŕs spent grain</mods:topic>
</mods:subject>
<mods:subject>
<mods:topic>Protein</mods:topic>
</mods:subject>
<mods:subject>
<mods:topic>Amino acids</mods:topic>
</mods:subject>
<mods:subject>
<mods:topic>Individual phenolic compounds</mods:topic>
</mods:subject>
<mods:subject>
<mods:topic>Antioxidant capacity</mods:topic>
</mods:subject>
<mods:titleInfo>
<mods:title>Subcritical water as hydrolytic medium to recover and fractionate the protein fraction and phenolic compounds from craft brewer’s spent grain</mods:title>
</mods:titleInfo>
<mods:genre>info:eu-repo/semantics/article</mods:genre>
</mods:mods>
</xmlData>
</mdWrap>
</dmdSec>
<amdSec ID="TMD_10259_5672">
<rightsMD ID="RIG_10259_5672">
<mdWrap OTHERMDTYPE="DSpaceDepositLicense" MDTYPE="OTHER" MIMETYPE="text/plain">
<binData>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</binData>
</mdWrap>
</rightsMD>
</amdSec>
<amdSec ID="FO_10259_5672_6">
<techMD ID="TECH_O_10259_5672_6">
<mdWrap MDTYPE="PREMIS">
<xmlData xmlns:premis="http://www.loc.gov/standards/premis" xsi:schemaLocation="http://www.loc.gov/standards/premis http://www.loc.gov/standards/premis/PREMIS-v1-0.xsd">
<premis:premis>
<premis:object>
<premis:objectIdentifier>
<premis:objectIdentifierType>URL</premis:objectIdentifierType>
<premis:objectIdentifierValue>https://riubu.ubu.es/bitstream/10259/5672/6/Alonso-Fc_2021.pdf</premis:objectIdentifierValue>
</premis:objectIdentifier>
<premis:objectCategory>File</premis:objectCategory>
<premis:objectCharacteristics>
<premis:fixity>
<premis:messageDigestAlgorithm>MD5</premis:messageDigestAlgorithm>
<premis:messageDigest>3d2a7d0adecf2a81dcc19ae6b8b35bee</premis:messageDigest>
</premis:fixity>
<premis:size>808043</premis:size>
<premis:format>
<premis:formatDesignation>
<premis:formatName>application/pdf</premis:formatName>
</premis:formatDesignation>
</premis:format>
</premis:objectCharacteristics>
<premis:originalName>Alonso-Fc_2021.pdf</premis:originalName>
</premis:object>
</premis:premis>
</xmlData>
</mdWrap>
</techMD>
</amdSec>
<amdSec ID="FT_10259_5672_5">
<techMD ID="TECH_T_10259_5672_5">
<mdWrap MDTYPE="PREMIS">
<xmlData xmlns:premis="http://www.loc.gov/standards/premis" xsi:schemaLocation="http://www.loc.gov/standards/premis http://www.loc.gov/standards/premis/PREMIS-v1-0.xsd">
<premis:premis>
<premis:object>
<premis:objectIdentifier>
<premis:objectIdentifierType>URL</premis:objectIdentifierType>
<premis:objectIdentifierValue>https://riubu.ubu.es/bitstream/10259/5672/5/Alonso-fc_2021.pdf.txt</premis:objectIdentifierValue>
</premis:objectIdentifier>
<premis:objectCategory>File</premis:objectCategory>
<premis:objectCharacteristics>
<premis:fixity>
<premis:messageDigestAlgorithm>MD5</premis:messageDigestAlgorithm>
<premis:messageDigest>f0d1f697764e6dba09202b3927cee2a3</premis:messageDigest>
</premis:fixity>
<premis:size>66471</premis:size>
<premis:format>
<premis:formatDesignation>
<premis:formatName>text/plain</premis:formatName>
</premis:formatDesignation>
</premis:format>
</premis:objectCharacteristics>
<premis:originalName>Alonso-fc_2021.pdf.txt</premis:originalName>
</premis:object>
</premis:premis>
</xmlData>
</mdWrap>
</techMD>
</amdSec>
<fileSec>
<fileGrp USE="ORIGINAL">
<file ID="BITSTREAM_ORIGINAL_10259_5672_6" MIMETYPE="application/pdf" SEQ="6" SIZE="808043" CHECKSUM="3d2a7d0adecf2a81dcc19ae6b8b35bee" CHECKSUMTYPE="MD5" ADMID="FO_10259_5672_6" GROUPID="GROUP_BITSTREAM_10259_5672_6">
<FLocat xlink:type="simple" LOCTYPE="URL" xlink:href="https://riubu.ubu.es/bitstream/10259/5672/6/Alonso-Fc_2021.pdf"/>
</file>
</fileGrp>
<fileGrp USE="TEXT">
<file ID="BITSTREAM_TEXT_10259_5672_5" MIMETYPE="text/plain" SEQ="5" SIZE="66471" CHECKSUM="f0d1f697764e6dba09202b3927cee2a3" CHECKSUMTYPE="MD5" ADMID="FT_10259_5672_5" GROUPID="GROUP_BITSTREAM_10259_5672_5">
<FLocat xlink:type="simple" LOCTYPE="URL" xlink:href="https://riubu.ubu.es/bitstream/10259/5672/5/Alonso-fc_2021.pdf.txt"/>
</file>
</fileGrp>
</fileSec>
<structMap TYPE="LOGICAL" LABEL="DSpace Object">
<div TYPE="DSpace Object Contents" ADMID="DMD_10259_5672">
<div TYPE="DSpace BITSTREAM">
<fptr FILEID="BITSTREAM_ORIGINAL_10259_5672_6"/>
</div>
</div>
</structMap>
</mets></metadata></record></GetRecord></OAI-PMH>