2024-03-29T15:31:52Zhttps://riubu.ubu.es/oai/requestoai:riubu.ubu.es:10259/62362022-11-09T12:25:36Zcom_10259_4244com_10259_5086com_10259_2604col_10259_4245
Extraction Optimization and Valorization of the Cornelian Cherry Fruits Extracts: Evidence on Antioxidant Activity and Food Applications
Enache, Iuliana Maria
Benito Román, Oscar
Coman, Gigi
Vizireanu, Camelia
Stănciuc, Nicoleta
Andronoiu, Doina Georgeta
Mihalcea, Liliana
Sanz Díez, Mª Teresa
Cornus mas
Antioxidants
Conventional extraction
Ultrasound-assisted extraction
Jelly candies
Ingeniería química
Alimentos
Chemical engineering
Food
In this work, the optimization of two extraction methods, conventional CE and ultrasound-assisted UAE, to obtain extracts from cornelian cherry fruit with high antioxidant activity, which can be used to produce healthier jelly candies, is presented. In the CE process, the effects of temperature (30–50 °C), time (15–45 min), and hydroalcoholic mixtures (60–100% ethanol, v/v) were studied. The highest antioxidant activity (29.83 ± 0.85 mg TE/g dw) was found in the extracts obtained using 60% ethanol at 40 °C for 15 min. The UAE process led to comparable values of 26.60 ± 0.53 mg TE/g dw at 40% amplitude and pulsed sonication (5 s on and 5 s off) for 12.5 min. Under these experimental conditions, the specific energy consumed was 1.91 kJ/g. The vitamin C content and its inhibitory activity against metabolic enzymes were evaluated in extracts with different antioxidant activity. A significant inhibitory effect against carbohydrate-metabolism-associated enzymes was identified for all the tested extracts, with an inhibitory effect against α-glucosidase higher than 75%, but with a lower effect against α-amylase. The extract obtained by CE (60% ethanol, 40 °C, 15 min) provided the highest vitamin C content of 39.9 ± 1.2 mg ascorbic acid/100 g dw. Four variants of the healthier jelly candies were formulated, with a vitamin C content of 0.34 mg ascorbic acid/100 g dw in samples with agar-agar and 0.70 mg ascorbic acid/100 g dw in samples with gelatin.
Romanian Ministry of Research and Innovation, CNCS-UEFISCDI, project numbers PN-III-P1-1.1-MC-2019-1905 and PN-III-P1-1.1-MC-2019-1908, within PNCDI III. The APC was funded by M.T.S. The authors are also grateful to Junta de Castilla y León (Spain) and ERDF for the financial support of project BU050P20. The Ó. Benito–Román post-doctoral contract was funded by Junta de Castilla y León (Spain) and ERDF through project BU050P20 and by Agencia Estatal de Investigación through project PID2020-116716RJ-I00/AEI/10.13039/501100011033.
2021-11-24T13:55:08Z
2021-11-24T13:55:08Z
2021-11
info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
2076-3417
http://hdl.handle.net/10259/6236
10.3390/app112210729
eng
Applied Sciences. 2021, V. 11, n. 22, 10729
https://doi.org/10.3390/app112210729
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PID2020-116716RJ-I00/ES/TECNOLOGIAS DE FLUIDOS PRESURIZADOS PARA LA VALORIZACION DE SUBPRODUCTOS DE LA INDUSTRIA AGROALIMENTARIA: RECUPERACION DE PECTINA Y OTROS COMPUESTOS BIOACTIVOS DE ALTO VALOR
info:eu-repo/grantAgreement/Junta de Castilla y León//BU050P20
info:eu-repo/grantAgreement/MCI//PN-III-P1-1.1-MC-2019-1905
info:eu-repo/grantAgreement/MCI//PN-III-P1-1.1-MC-2019-1908
Atribución 4.0 Internacional
http://creativecommons.org/licenses/by/4.0/
info:eu-repo/semantics/openAccess
application/pdf
MDPI