RT dataset T1 Dataset of the work “Multiamperometric-SERS detection of melamine on gold screen-printed electrodes” A1 Hernández Muñoz, Sheila A1 García, Lydia A1 Pérez Estébanez, Martín A1 Cheuquepan Valenzuela, William A1 Heras Vidaurre, Aránzazu A1 Colina Santamaría, Álvaro K1 EC-SERS K1 Gold-electrodes K1 Time-resolved spectroelectrochemistry K1 Raman K1 Melamine K1 Química analítica K1 Chemistry, Analytic AB A new, simple and fast protocol to generate gold-based SERS substrates is presented in this work. Melamine is a compound widely used in the industry that can be toxic for humans if consumed even in low concentrations. EC-SERS is an excellent alternative to classical methods to detect and quantify this compound because Raman spectroscopy provides a fingerprint of the molecules, providing very good sensitivity. In this work, time-resolved Raman spectroelectrochemistry is employed to generate a SERS substrate and to detect melamine, all in a single experiment. The dynamic character of this technique provides valuable information about the interaction of the molecule with the generated substrate. An optimization of the spectroelectrochemical method based on a multi-pulse amperometric detection has been performed. The new protocol presented in this work shows significant figures of merit in a very short experiment time, just 25 s. PB Universidad de Burgos YR 2023 FD 2023-05-29 LK http://hdl.handle.net/10259/7682 UL http://hdl.handle.net/10259/7682 LA eng NO Hernández Muñoz, Sheila; Garcia, Lydia; Pérez Estébanez, Martín; Cheuquepan Valenzuela, William, Heras Vidaurre, Aránzazu; Colina Santamaría, Álvaro; 2023; Dataset of the work “Multiamperometric-SERS detection of melamine on gold screen-printed electrodes”; RIUBU; http://doi.org/10.36443/10259/7682 NO Authors acknowledge the financial support from Agencia Estatal de Investigación/Ministerio de Ciencia e Innovacion /10.13039/501100011033 (Grant PID2020-113154RB-C21) and Ministerio de Ciencia, Innovación y Universidades (Grant RED2018-102412-T). W. Ch. thanks JCyL for his postdoctoral fellowship (Grant BU297P18). S.H. and M.P-E. thank JCyL and European Social Fund for their predoctoral fellowships. DS Repositorio Institucional de la Universidad de Burgos RD 03-may-2024