Por favor, use este identificador para citar o enlazar este ítem: https://hdl.handle.net/10259/11443
Título
Consistent DSC and TGA Methodology as Basis for the Measurement and Comparison of Thermo-Physical Properties of Phase Change Materials
Autor
Publicado en
Materials. 2020, V. 13, n. 20, p. 4486-4506
Editorial
MDPI
Fecha de publicación
2020-10
DOI
10.3390/ma13204486
Résumé
Measuring thermo-physical properties of phase change materials (PCM) in a consistent and reliable manner is essential for system layout of thermal energy storages and correspondingly material selection. Only if basic properties are assessed in a comparable way a selection process leads to the top candidate for any given application and thus enhances market penetration of renewable energy sources coupled with thermal energy storage. In this study, we focus on differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) as basic assessment techniques and develop consistent measurement procedures to create a database with comparable results. We show consistency of the measured results through analysis of coefficient of variation (CV), being in the mean 1.69%, 0.05%, 0.06% and 4.00% for enthalpy, melting onset, melting peak and maximum operating temperature, respectively. Overall, 23 PCM have been measured with the presented methodology, which was mainly possible due to the reduced measurement and preparation time per PCM compared to standard techniques, while achieving similar accuracy and precision.
Palabras clave
Phase change materials
Latent heat storage
Thermal energy storage
Differential scanning calorimetry
Thermogravimetric analysis
Energy
Materia
Ingeniería Química
Chemical engineering
Termodinámica
Thermodynamics
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