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    Por favor, use este identificador para citar o enlazar este ítem: http://hdl.handle.net/10259/4528

    Título
    Molybdenum-catalyzed deoxygenation of heteroaromatic n-oxides and hydroxides using Pinacol as Reducing Agent
    Autor
    Rubio Presa, RubénUBU authority
    Fernández Rodríguez, Manuel A.UBU authority
    Pedrosa Sáez, María de los RemediosUBU authority
    Arnáiz García, Francisco JavierUBU authority
    Sanz Díez, RobertoUBU authority
    Publicado en
    Advanced Synthesis & Catalysis. 2017, V. 359, n. 10, p. 1752–1757
    Editorial
    Wiley-VCH Verlag
    Fecha de publicación
    2017-05
    ISSN
    1615-4150
    DOI
    10.1002/adsc.201700071
    Abstract
    A molybdenum-catalyzed deoxygenationof pyridine N -oxides and N-hydroxybenzotriazoles,as well as other azole N-oxides, has been developedusing pinacol as an environmentally friendly oxo-acceptor. The only by-products are acetone andwater making the process a convenient alternativeto established protocols in terms of waste gener-ation. The reaction is highly chemose lective and avariety of functional groups are tolerated. Theprocesses are usually very clean allowing theisolation of the pure deoxygenated products after asimple extraction in most cases.
    Palabras clave
    amine N-oxides
    deoxygenation
    molyb-denum
    microwave heating
    N-hydroxybenzotria-zoles
    Materia
    Química orgánica
    Chemistry, Organic
    URI
    http://hdl.handle.net/10259/4528
    Versión del editor
    http://dx.doi.org/10.1002/adsc.201700071
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